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The main instrumentation in the facility, a Mass Analyser
Products 215-50 noble gas mass-spectrometer and its associated
ultra-high vacuum extraction line, became fully operational
in May 1997.
The mass spectrometer is an extended geometry 90° sector
E.S.A. equipped with a Nier-type source and a dual collector
system (a Faraday detector and a BalzersTM, 217
electron multiplier). The signal from the electron multiplier
is further amplified through a KeithleyTM, 6512
Electrometer, which increases the dynamic range of signals
analysed.
The system is fully automated. The ultra-high vacuum extraction
line is equipped with two independent heating sources, a
Coherent 10W continuous Ar-ion laser and a custom built,
Berkeley-type, resistance furnace.
The laser extraction line is further equipped with NewportTM,
stepper- motors and an MM3000 motion controller which allows
for the pre-programming of step- heating analyses of up
to 221 samples. The sample chamber is continuously monitored
through a SonyTM, CCD camera and the image is
viewed in a SonyTM, Trinitron monitor. Recording
of sample heating is possible through a SonyTM,
video-cassette recorder.
Laser-heating experiments are ideally suited to the analyses
of very small samples and of very young samples. The high
spatial resolution of this heating technique results in
intrinsically low blanks. Laser- heating is also very fast
and is ideal for geochron- ological applications where heating
temperatures do not need to be known. If precise temperature
measurements are necessary, the sample can be heated in
a double-vacuum 600A-5V resistance furnace equipped with
a molybdenum crucible, a niobium heating element, and a
custom designed automated loading device capable of handling
up to 20 samples.
The laser, resistance furnace, and extraction line gas
flow is fully automated through Mass Spec, a Macintosh-based
software developed by Al Deino, from the Berkeley
Geochronology Center, Berkeley, Ca.
The whole system is controlled through a Power Macintosh
7100/80 computer. On-line data collection, analyses, and
interpretation are also carried-out during normal operation.
A Macintosh 7600/132 computer is used for off-line data
correction, interpretation, and plotting.
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